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Beilstein J. Org. Chem. 2016, 12, 245–252, doi:10.3762/bjoc.12.26
Graphical Abstract
Figure 1: Schematic representation of a deprotection taking the relatively high polarity of the transition st...
Scheme 1: Synthesis of Br-t-Boc-protected monomers 3a,b and homopolymers 6a,b.
Figure 2: 300 MHz 1H NMR spectrum of 3a in CDCl3.
Figure 3: 300 MHz 1H NMR spectrum of 3b in CDCl3.
Scheme 2: Stability of 3 in different solvents.
Scheme 3: Synthesized derivative monomers 3c,d.
Scheme 4: a) Self deactivation of homopolymer 6a,b due to competing hydrogen interactions in comparison to b)...
Figure 4: Kinetic studies of the deprotection of 3a, 6a and 7a.
Figure 5: 300 MHz 1H NMR spectra of a) 6a in CDCl3 and b) 8a in DMSO-d6.